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Organically Modified Metal Alkoxide Precursors
01.06.2008 - 31.05.2011
Research funding project
In many sol-gel protocols, metal alkoxides are reacted in situ with chelating organic ligands. Despite the fact that substituting one or more OR groups by such ligands has huge impact on the formation, structure and properties of the derived gels, the organically modified derivatives were rarely isolated or characterized. The goal of the project is to gain deeper insight into the basic reactivity and structural chemistry of organically modified metal alkoxides. The key issues to be investigated will be (i) the basic chemistry of organically modified metal alkoxides with focus on rarely used but promising ligands (such as oximes, hydroxamic acids, amino acids, ß-ketoimines or oxine derivatives) and a range of different metal alkoxides, (ii) the hydrolysis reactions of such derivatives by isolating and structurally characterizing partially hydrolyzed compounds and spectroscopic in-situ investigation of the hydrolysis reactions, and (iii) preparation on metal alkoxide derivatives with various functional organic ligands. The vision is that it may be possible in the future to design sol-gel materials by assembling tailor-made molecular building blocks in a rational way to achieve a particular set of materials properties. In order to do so, a collection of different building blocks with different shapes (structures), functionalities, connectivities, etc. must be readily available and their reactivity must be mastered. The knowledge gained in the project will be a step forward in this direction.
People
Project leader
Ulrich Schubert
(E165)
Project personnel
Stefan Baumann
(E165)
Rupali Ganpat Deshmukh
(E165)
Robert Lichtenberger
(E165)
Marco Litschauer
(E165)
Miroslava Malenovska
(E165)
Christian Maurer
(E165)
Institute
E165 - Institute of Materials Chemistry
Grant funds
FWF - Österr. Wissenschaftsfonds (National)
Austrian Science Fund (FWF)
Research focus
Non-metallic Materials: 80%
Structure-Property Relationsship: 20%
Keywords
German
English
Precursorchemie
Precursor chemistry
Sol-Gel Prozess
sol-gel processing
Metall-Alkoxide
Metal alkoxides
Organofunktionelle Derivate
Organofunctional derivatives
Publications
Publications