1.) EXERCISE REGISTRATION VIA TISS REQUIRED!
2.) MANDATORY PARTICIPATION IN THE ON-LINE INTERNSHIP INTRODUCTION TEST! (TUE October 3rd, 2023, 6:00 p.m. - 8:00 p.m., Zoom event) if the LVA 165.008 "Physical Chemistry LU" has not yet been successfully completed.
3.) REGISTRATION FOR THE ON-LINE INTERNSHIP INTRODUCTION TEST! If you want to take part in the online internship introductory test, you must register for the online internship introductory test! (Registration in TISS under exams)
4.) MANDATORY PARTICIPATION IN THE ON-LINE INFORMATION EVENT. The laboratory training places will be assigned on Thursday, October 5th, 2023 at 6:00 a.m. as part of a Zoom event (invitation will be sent to registered students in good time via TISS). Please have your student ID ready and show it into the camera when asked. The certificate from LVA 165.008 “Physical Chemistry LU” must also be held up to the camera when requested.
5.) MANDATORY PARTICIPATION IN THE SAFETY INTRODUCTION IN PRESENCE: THU 10/5/2023 (see registration in TISS under exams)
6.) START OF LABORATORY EXERCISES: MON 10/9/2023
Information about the online internship introductory test: Registration for the online internship introductory test must be made in TISS (under exams)! It will be held as a Zoom event. The online internship introductory test will include two calculation examples. The material tested during the introductory internship test for laboratory exercises 166.209 covers the following subject areas: 1. Ideal gases and gas mixtures (Dalton, Raoult, conversions: vol.-%, m.-%, mol-%...), 2. Real gases (van der Waals, critical state variables), 3. Liquids, solutions and mixtures (Clausius and Clapeyron, equation of August, Raoult, Nernst distribution theorem, Henry, activity and activity coefficient), 4. Gas equilibria (mass distribution law according to Guldberg and Libra, Concentration information, partial pressures, Le Chatelier and Braun, van t Hoff equations), 5. Electrolyte equilibria (osmotic pressure, pH value, degree of hydrolysis, activity), 6. First law of thermodynamics (enthalpy of reaction, isobaric, isothermal, adiabatic volume change , isochoric processes, Dulong and Petit, Hess theorem, Kirchhoff theorem), 7. Second law of thermodynamics (reaction entropy, Gibbs free energy), 8. Reaction kinetics (first and second order reactions, Arrhenius equation).
Literature: K.H. Näser "Physical-chemical calculation tasks", VEB German publisher for basic industry, Leipzig
The results of the online internship introductory test (TUE October 3rd, 2023, 6:00 p.m. - 8:00 p.m., Zoom event) will be announced to the participants by email from the TISS system after the test! Rating: E with success; O without success. If the online internship introductory test was graded O, an application for a laboratory training place on Thursday, October 5th, 2023 at 6:00 a.m. is not possible!
The TUWEL course "Verfahrenstechnik I Labor WS 2023/24" was set up to organize the lecture. Access is possible when students are admitted to the LVA.
The internship must be completed by January 23, 2024, otherwise the student must repeat the entire internship.
The 10 individual exercises are carried out in groups of two students each. An individual exercise includes: a preliminary discussion (in presence, Tuwel registration required), the practical exercise part (in presence, Tuwel registration required), the preparation of a protocol (Tuwel submission), a final debriefing by the respective supervisor (in presence, Tuwel registration required). The appointment for the preliminary discussion and the appointment for the experimental exercise part must be in the same calendar week. The practical exercise part takes place in person in the institute's main laboratory (BI, 4th floor). The groups of two choose the dates themselves in Tuwel.
Access to the Tuwel course is activated when the student is admitted to the LVA (THU 05.10.2023, from 6:00 a.m.).
The preliminary discussion for each individual exercise takes place before the practical part of the exercise. Attendance at the preliminary meeting is mandatory for both exercise participants. Registration for the preliminary meeting takes place in Tuwel.
The preliminary discussion can also be carried out in writing. An internet-capable computer is necessary.
The chapter “Measurement technology” in the laboratory exercise script can be checked at every preliminary meeting. There is no practical exercise section on “Measurement technology”.
The exercise groups determine their own exercise days by registering for the practical exercise part of the Tuwel course. All partial exercises are carried out in person in the institute's main laboratory. For this purpose, the group members meet at the training apparatus in the main laboratory and are introduced to the exercise by the supervisor.
For each exercise group, a protocol containing the name of the supervisor, the date of the practical exercise part and the names of the group members must be submitted to the responsible supervisor by submitting it to the Tuwel course no later than two weeks after the practical exercise was carried out, otherwise a grade deterioration occurs.
The exercise group must appear for a debriefing with the supervisor no later than the second Monday after the practical exercise part. The debriefing dates can be found in the Tuwel course. Attendance at the debriefing is mandatory for both group members.
The certificate is issued at the end of the semester. All students who have not completed the laboratory exercises by the end of the semester will receive a negative certificate and must complete the laboratory exercises again.
There will be no excursion.
The documents required to carry out the laboratory exercise will be made available to all participants in the TISS under Communication. For the preliminary discussion, please refer to the relevant literature.
Each individual exercise is graded by the supervisor (S1 – N5). The certificate grade is the average of the grades of the individual exercises.
The laboratory exercise is considered to have been completed negatively if: the one-semester deadline is exceeded, if an individual exercise was assessed negatively and if an unexcused absence from an individual exercise occurs.
The relevant safety regulations of the TU Vienna must be adhered to!
All students participating in this course are required to attend one of the listed safety introductions in person. (see TISS registration under exams)!
Personal protective equipment (lab coat, safety glasses) must be provided by the student.
Lecture notes for this course are available.
Mauschitz G. Literature for lecture Mechanical Process Engineering I 159.478;
Friedl A.: Literature for lecture Thermal Process Engineering I 159.731;
Reichhold A.: Literature for lecture Chemical Process Engineering 159.786;
Vauck W. R. A. und Müller H. A.: Grundoperationen chemischer Verfahrenstechnik, 9. Auflage, Deutscher Verlag für Grundstoffindustrie GmbH, Leipzig, 1992.
Sattler K.: Thermische Trennverfahren, 2. überarbeitete Auflage, VCH, Weinheim, 1995.
Autorenkollektiv: Lehrbuch der chemischen Verfahrenstechnik, 5. bearbeitete Auflage, VEB Deutscher Verlag für Grundstoffindustrie, Leipzig, 1983.
Ullmanns Enzyklopädie der Technischen Chemie, hrsg. von Ernst Barholomé, Band II, 4., neubearb. u. erw. Aufl., Verlag Chemie, Weinheim.
Stieß Matthias: „Mechanische Verfahrenstechnik - Partikeltechnologie 1“, 3. vollständig neu bearbeitete Auflage, Springer-Verlag Berlin, Heidelberg, 2009, 498S., ISBN 978-3-540-32551-2
Stieß Matthias: „Mechanische Verfahrenstechnik 2“,Springer-Verlag Berlin, Heidelberg, 1997, 407S., ISBN 3-540-55852-7
Schubert Heinrich: „Handbuch der Mechanischen Verfahrenstechnik Band 1“, WILEY-VCH Weinheim, 2003, 498S., ISBN 978-3-527-30577-3
Schubert Heinrich: „Handbuch der Mechanischen Verfahrenstechnik Band 2“, WILEY-VCH Weinheim, 2003, 1271S., ISBN 978-3-527-30577-3
Zogg Martin: „Einführung in die Mechanische Verfahrenstechnik“, 3. überarbeitete Auflage, B. G. Teubner Stuttgart, 1993, 269S., ISBN 3-519-16319-5 I
Müller Walter: "Mechanische Verfahrenstechnik und ihre Gesetzmäßigkeiten", 2. Auflage, Oldenbourg Wissenschaftsverlag München, 2014, 316S., ISBN 978-3-11-034344-1
