165.008 Physical Chemistry, Laboratory Course
This course is in all assigned curricula part of the STEOP.
This course is in at least 1 assigned curriculum part of the STEOP.

2020W, LU, 9.0h, 9.0EC, to be held in blocked form
TUWEL
This course is evaluated following the new mode. Learn more

Course evaluation

Properties

  • Semester hours: 9.0
  • Credits: 9.0
  • Type: LU Laboratory Exercise
  • Format: Hybrid

Learning outcomes

After successful completion of the course, students are able to apply theoretical knowledge acquired in the basic lecture of physical chemistry in practical experiments, either independently or in groups, as well as to perform data analysis, evaluation and error analysis (standard deviation, outlier tests and error propagation) and to create measurement reports.

Subject of course

Practical course in Physical chemistry and physics

Practice examples from the chapters are given:

A. Ideal/real gases: 1. molar mass according to Dumas; 2. Joule-Thomson effect.

B. State changes: 1. critical point and vapour pressure determination; 2. boiling diagram; 3. melting diagram; 4. Cryoscopy.

C. Determination of thermodynamic parameters: 1st calorimeter: Precipitation and combustion reaction; 2. heat pump: Stirling engine, Peltier and Seebeck effect; 3. electrochemical cells and solar cells.

D. Physical and chemical equilibria: 1. adsorption; 2. surface tension; 3. acid-base equilibria; 4. distribution between two phases.

E. Kinetics: 1. cane sugar inversion (polarimeter); 2. ester saponification (conductivity or titration).

F. Transport phenomena: 1. diffusion; 2. measurement of the electrical conductivity of electrolyte solutions; 3. vacuum technique; 4. Viscosity.

G. Structure, quantum mechanics and natural constants: 1. dipole meter; 2. emission spectra of atoms; 3. photo effect; 4. Franck-Hertz experiment; 5. millikan experiment; 6. X-ray diffractometer.

Teaching methods

Execution of individual exercises at different test stations:

e.g. Dipolemeter, vapor pressure apparatus, calorimeter, Kofler microscope, etc.

This includes the e.g. measurement of current and voltage, pressure, pH value, refractive index, viscosity, etc.

Execution of error analysis for the individual results obtained

Mode of examination

Immanent

Additional information

Als Aufnahmekriterium wird das positive Zeugnis über die Vorlesung "Physikalische Chemie I" (165.003 bzw. 165.098)) verlangt. ANWESENHEITSPFLICHT bei der Vorbesprechung/Einführung zur LU.

Übersteigt die Zahl der Anmeldung die Zahl der verfügbaren Laborplätze und wird damit eine Reihung der angemeldeten Studierenden mit erfüllter Eingangsvoraussetzung notwendig, so gelten folgende Reihungskriterien:

Reihungskriterium 1: Positiv abgelegte Mathematik für TCH I Prüfung (104.084)

(Datum und Note der Prüfung ist KEIN Kriterium)

Reihungskriterium 2: Datum der positiv abgelegten PCI Prüfung (165.098)

Reihungskriterium 3: Note der PCI Prüfung (165.098)

Reihungskriterium 4: Datum der Mathematik für TCH I Prüfung (104.084)

Reihungskriterium 5: Note der Mathematik für TCH I Prüfung (104.084)


! For data protection purposes we can only respond to enquiries sent from an official TU (student) e-mail address !


Lecturers

Institute

Course dates

DayTimeDateLocationDescription
Fri11:00 - 12:0009.10.2020 Virtuell Via Zoom: https://tuwien.zoom.us/j/99781903728?pwd=YkY4ZkVjaVdoT0xCRzdmZTg0eHhpQT09 Passwort: LU165.008Kurs 1: Sicherheit, Organisation und Durchführung - Anwesenheitspflicht Kurs 1 - Rameshan, Buhr
Fri13:00 - 17:0009.10.2020 Virtuell Via Zoom https://tuwien.zoom.us/j/97769390699?pwd=Q2JKbGMvY2graW9vTXVJallaVEI0QT09 Password: LU165.008Kurs 1 - Vorversuche (Online Vortrag) Teilnahmepflicht!
13:00 - 18:0012.10.2020 - 16.11.2020 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Fri11:00 - 12:0013.11.2020 Virtuell Via Zoom https://tuwien.zoom.us/j/99261635599?pwd=Zlcyem9aQXVBVWtZaktYVHA2Nm5Mdz09 Passwort:LU165.008Kurs 2: Sicherheit, Organisation und Durchführung - Anwesenheitspflicht Kurs 2 - Rameshan, Buhr
Fri13:00 - 17:0013.11.2020 Virtuell Via Zoom https://tuwien.zoom.us/j/94513501488?pwd=eXd5c0VDKzRJanRaK0FsbGhveEZMQT09 Passwort:LU165.008Kurs 2 - Vorversuche (Online Vortrag) Teilnahmepflicht!
13:00 - 18:0017.11.2020 - 18.12.2020 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 2: Versuche - Rameshan
Physical Chemistry, Laboratory Course - Single appointments
DayDateTimeLocationDescription
Fri09.10.202011:00 - 12:00 Virtuell Via Zoom: https://tuwien.zoom.us/j/99781903728?pwd=YkY4ZkVjaVdoT0xCRzdmZTg0eHhpQT09 Passwort: LU165.008Kurs 1: Sicherheit, Organisation und Durchführung - Anwesenheitspflicht Kurs 1 - Rameshan, Buhr
Fri09.10.202013:00 - 17:00 Virtuell Via Zoom https://tuwien.zoom.us/j/97769390699?pwd=Q2JKbGMvY2graW9vTXVJallaVEI0QT09 Password: LU165.008Kurs 1 - Vorversuche (Online Vortrag) Teilnahmepflicht!
Mon12.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Tue13.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Wed14.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Thu15.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Fri16.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Mon19.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Tue20.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Wed21.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Thu22.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Fri23.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Tue27.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Wed28.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Thu29.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Fri30.10.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Tue03.11.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Wed04.11.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Thu05.11.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Fri06.11.202013:00 - 18:00 Hörerlabor Lehar 4/5 (Raumnummer BC04 H31/41)Kurs 1: Versuche - Rameshan
Course is held blocked

Examination modalities

You must successfully complete 10 exercises (it is not possible to skip exercises). Each exercise consists of: Preliminary discussion, execution, writing of minutes and debriefing. For each exercise there is a maximum of 10 points. (total number of points max. 100). The grade of the laboratory exercise is calculated from the total number of points of all exercises (see grading scale). The points for the partial exercises will be awarded according to the following scale: 3 points for preliminary discussion, 4 points for protocol, 3 points for debriefing + experiment execution. A sub-exercise is considered successfully passed if at least 5 points are achieved.

 

grading scheme

Very good:                  89 - 100

Good:                          77 - 88

Satisfactory:               64 - 76

Sufficient:                   51 - 63

Unsatisfactory:          0 – 50

 

Attendance is compulsory for all members of a group until the end of the experiment. Failure to comply with the obligation to attend will result in the student being deprived of the day/part of the exercise and a retry must be made.

 

During the course of the course a maximum of 2 negative performances may be achieved (partial exercises not accomplished). These must then be corrected by retries (new partial exercises).

 

Only a maximum of 2 retries are possible. (In case of a self-caused retries there will be a 50% point reduction). If these 2 retries are not enough to complete the course, the course must be repeated.

 

Protocol submission: 10 working days after completion of the exercise (working days = Mon-Fri; Sat, Sun and public holidays do not count)

1.protocol submission will be evaluated (caution: Points will be deducted if the protocol is faulty/inadequate). Only if the assistant approves the protocol, a debriefing can be made.

The whole group is responsible for each protocol (group liability)! If you have any questions about the protocol, please contact the respective assistant before the deadline.

 

If the protocol is submitted late, it will not be accepted and a retry must be made! Inadequate protocols or major misconduct (e.g. endangering others) in the laboratory can also lead to retries.

 


Course registration

Begin End Deregistration end
10.07.2020 00:00 11.11.2020 17:59 13.11.2020 11:59

Registration modalities:

Die Vorbesprechung Einführung in die PC Laborübung ist Aufnahmevoraussetzung (ohne Ausnahme)! Verspätung gilt als Nichterscheinen!

Im Zuge der Vorbesprechung werden Sie weitere Einzelheiten erfahren.

Precondition

The student must have at least 1 of the course(s) completed listed below:

Group Registration

GroupRegistration FromTo
A 1 fertig15.09.2020 00:0015.09.2020 00:01
A 2 fertig15.09.2020 00:0015.09.2020 00:01
A 315.09.2020 00:0015.09.2020 00:01
A 4 fertig15.09.2020 00:0015.09.2020 00:01
A 5 fertig15.09.2020 00:0015.09.2020 00:01
A 615.09.2020 00:0015.09.2020 00:01
A 7 fertig15.09.2020 00:0015.09.2020 00:01
A 8 fertig15.09.2020 00:0015.09.2020 00:01
B 1 fertig15.09.2020 00:0015.09.2020 00:01
B 2 fertig+15.09.2020 00:0015.09.2020 00:01
B 3 fertig15.09.2020 00:0015.09.2020 00:01
B 415.09.2020 00:0015.09.2020 00:01
B 5 fertig15.09.2020 00:0015.09.2020 00:01
B 6 50% fertig15.09.2020 00:0015.09.2020 00:01
B 7 fertig15.09.2020 00:0015.09.2020 00:01
B 8 fertig15.09.2020 00:0015.09.2020 00:01
C 115.09.2020 00:0015.09.2020 00:01
C 215.09.2020 00:0015.09.2020 00:01
C 3 fertig15.09.2020 00:0015.09.2020 00:01
C 4 fertig15.09.2020 00:0015.09.2020 00:01
C 515.09.2020 00:0015.09.2020 00:01
C 615.09.2020 00:0015.09.2020 00:01
C 7 fertig15.09.2020 00:0015.09.2020 00:01
D 1 fertig15.09.2020 00:0015.09.2020 00:01
D 215.09.2020 00:0015.09.2020 00:01
D 3 fertig15.09.2020 00:0015.09.2020 00:01
D 4 fertig15.09.2020 00:0015.09.2020 00:01
D 5 fertig15.09.2020 00:0015.09.2020 00:01
D 615.09.2020 00:0015.09.2020 00:01
D 715.09.2020 00:0015.09.2020 00:01
E 118.09.2020 00:0018.09.2020 00:01
E 2 fertig18.09.2020 00:0018.09.2020 00:01
E 318.09.2020 00:0018.09.2020 00:01
E 418.09.2020 00:0018.09.2020 00:01
E 518.09.2020 00:0018.09.2020 00:01
E 618.09.2020 00:0018.09.2020 00:01
E 718.09.2020 00:0018.09.2020 00:01
F 125.09.2020 00:0025.09.2020 00:01
F 225.09.2020 00:0025.09.2020 00:01
F 3 fertig25.09.2020 00:0025.09.2020 00:01
F 425.09.2020 00:0025.09.2020 00:01
F 525.09.2020 00:0025.09.2020 00:01
F 625.09.2020 00:0025.09.2020 00:01
F 725.09.2020 00:0025.09.2020 00:01
G 125.09.2020 00:0025.09.2020 00:01
G 225.09.2020 00:0025.09.2020 00:01
G 325.09.2020 00:0025.09.2020 00:01
G 425.09.2020 00:0025.09.2020 00:01
G 525.09.2020 00:0025.09.2020 00:01
G 625.09.2020 00:0025.09.2020 00:01
G 725.09.2020 00:0025.09.2020 00:01
H 125.09.2020 00:0025.09.2020 00:01
H 225.09.2020 00:0025.09.2020 00:01
H 325.09.2020 00:0025.09.2020 00:01
H 425.09.2020 00:0025.09.2020 00:01
H 525.09.2020 00:0025.09.2020 00:01
H 625.09.2020 00:0025.09.2020 00:01
H 725.09.2020 00:0025.09.2020 00:01

Curricula

Study CodeSemesterPrecon.Info
033 290 Technical Chemistry 5. SemesterSTEOP
Course requires the completion of the introductory and orientation phase

Literature

Previous knowledge

 

 

Miscellaneous

  • Attendance Required!

Language

German