163.176 Structure elucidation
This course is in all assigned curricula part of the STEOP.
This course is in at least 1 assigned curriculum part of the STEOP.

2019W, SE, 1.0h, 1.0EC, to be held in blocked form

Properties

  • Semester hours: 1.0
  • Credits: 1.0
  • Type: SE Seminar

Learning outcomes

After successful completion of the course, students are able to analyze the signals of NMR, IR, and mass spectra of a compound, deduce structural elements, combine these to a complete structure, and verify this result by cross-checking in all spectra.

Subject of course

Practical examples for structure elucidation of unknown molecules based on proton and carbon NMR spectra, IR spectra and electron impact mass spectra, discussion of convergent strategies for structure determination incorporating the following data: chemical shift-/coupling-/integration-information derived from NMR spectra; electron impact mass spectra: molecular weight and fragmentation, isotopic pattern, elemental composition and collisions induced dissociation; vibration types and frequencies as well as spectral ranges for various functional groups in IR spectroscopy; if required including data from chemical elemental analysis and utilization of computer-aided methods and data bases in NMR, IR and MS.

Teaching methods

Presentation of important aspects of NMR and IR spectroscopy as well as mass spectrometry by the lecturers; joint solving of combined spectral examples by lecturers and students.

Mode of examination

Written

Additional information

Please consider the plagiarism guidelines of TU Wien when writing your seminar paper: https://www.tuwien.ac.at/fileadmin/t/ukanzlei/t-ukanzlei-english/Plagiarism.pdf
Please consider the plagiarism guidelines of TU Wien when writing your seminar paper: https://www.tuwien.at/fileadmin/Assets/dienstleister/Datenschutz_und_Dokumentenmanagement/Plagiarism.pdf

Lecturers

Institute

Course dates

DayTimeDateLocationDescription
Tue09:00 - 11:0007.01.2020 - 28.01.2020GM 5 Praktikum HS SE Strukturaufklärung
Mon09:00 - 11:0013.01.2020 - 27.01.2020GM 5 Praktikum HS SE Strukturaufklärung
Structure elucidation - Single appointments
DayDateTimeLocationDescription
Tue07.01.202009:00 - 11:00GM 5 Praktikum HS SE Strukturaufklärung
Mon13.01.202009:00 - 11:00GM 5 Praktikum HS SE Strukturaufklärung
Tue14.01.202009:00 - 11:00GM 5 Praktikum HS SE Strukturaufklärung
Mon20.01.202009:00 - 11:00GM 5 Praktikum HS SE Strukturaufklärung
Tue21.01.202009:00 - 11:00GM 5 Praktikum HS SE Strukturaufklärung
Mon27.01.202009:00 - 11:00GM 5 Praktikum HS SE Strukturaufklärung
Tue28.01.202009:00 - 11:00GM 5 Praktikum HS SE Strukturaufklärung
Course is held blocked

Examination modalities

Written examination including three theoretical questions as well as one combined spectral example.

Exams

DayTimeDateRoomMode of examinationApplication timeApplication modeExam
Mon11:00 - 13:0003.02.2020GM 1 Audi. Max. written08.01.2020 00:01 - 30.01.2020 23:59TISSPrüfung
Wed14:00 - 16:0026.02.2020GM 2 Radinger Hörsaal written04.02.2020 00:01 - 24.02.2020 23:59TISSPrüfung
Fri16:00 - 18:0020.03.2020GM 2 Radinger Hörsaal written21.02.2020 00:01 - 16.03.2020 23:59TISSPrüfung
Fri14:00 - 16:0005.06.2020GM 2 Radinger Hörsaal written24.04.2020 00:01 - 01.06.2020 23:59TISSPrüfung

Course registration

Begin End Deregistration end
07.10.2019 00:00 07.02.2020 23:59

Curricula

Study CodeSemesterPrecon.Info
033 290 Technical Chemistry 3. Semester

Literature

No lecture notes are available.

Miscellaneous

  • Attendance Required!

Language

German