Ability to synthesize and characterize organic, inorganic and organometallic compounds according to given experimental instructions.
Syntheses and characterisations of organic and inorganic compounds by different mechanisms and diverse techniques. Experimental tasks are organized in thematic groups which contain methodologically similar examples; out of these the lab course of each student is compiled. This program comprises the syntheses of organic compounds by nucleophilic or radical substitution, addition or elimination, oxidation or reduction, substitution of aromatic compounds, condensation, diazotation as well as carbonyl- or carboxyl-derivative. One of these syntheses has to be done on small scale. In the inorganic part selected compound classes in inorganic and metalorganic chemistry are synthesized: simple metal complexes, molecular organic compounds of the main group elements, application of Li- and Mg-organyls in inorganic chemistry, metal organic compounds containing transition metals (metal carbonyls, sandwich complexes etc.). Further a natural product is isolated, a reaction with an organometallic compound is performed, a recombinant biocatalyst has to be prepared and to be used for an enzyme-catalyzed reaction, as well as a polymer has to be synthesized. Characterisation of all products is accomplished by appropriate spectroscopic methods and/or chromatography. Further important points are consciousness of environmental aspects and disposal of by-products. There is a discussion held prior to each synthesis. ECTS-credits are allocated to the particular topics as follows: Inorganic Chemistry - 6 credits, Organic Chemistry - 9 credits, Biochemistry - 1 credit and Macromolecular Chemistry - 1 credit.
FINDET NICHT MEHR STATT Einführungsvortrag: Dienstag, den 21.4.2009 von 11.00-14.00 Uhr im Chemie-HS Platzübernahme: Donnerstag, 23.4.2009 um 10.00 Uhr und 13.00 Uhr, Freitag, 24.4.2009 um 10.00 Uhr und 13.00 Uhr Beginn: Montag, 27.4.2009 Ende: Dienstag, 30.6.2009 Arbeitszeit: Montag jeweils von 9.00-16.30 Uhr, Dienstag bis Freitag jeweils von 10.00-18.00 Uhr ANMELDESCHLUSS: Dienstag, 31.3.2009
Abschlussbesprechung
Fire protection exercise Lecture 165.087 Inorganic Chemistry I Lecture 163.119 Organc Chemistry 1 and Lecture 172.695 Biochemistry I (can be substituted by a written exam about chapters 2-6 and 10-12 of the lecture; questions are the same as the ones for the lecture (corresponding chapters); the exam can be taken anytime after contacting Prof. Kubicek (about one week in advance)) have to be positively passed before the start of the laboratory course.
